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21.
《Ceramics International》2020,46(3):3144-3165
The ceramic nanocomposites (CNCs) like zirconia toughened alumina (ZTA) ceramics are important futuristic materials for structural and functional applications in advanced strategic systems, structural components, biomedical prostheses and devices. In all structural materials including the ZTA CNCs, the very early stages of plastic deformation i.e., the incipient plasticity events (IPE) are most important to be understood so that the microstructure and mechanical properties can be tuned to suit a given end application. Here we report for the first time the mechanisms of IPE in the nanoindentation experiments conducted at 10–1000 mN loads in the 40 ZTA CNCs. Here 40 ZTA CNC stands for 40 vol% of 3 mol% Yttria partially stabilized zirconia toughened alumina (40ZTA) CNC. The role of load ranges in variations of the IPE related parameters in the 40 ZTA CNCs is also studied. Further, an attempt is made to assess how the amount of zirconia content in ZTA CNCs affects the variations of the IPE related parameters. Through the extensive usage of field emission scanning electron microscopy (FESEM) and theoretical estimations, efforts are also directed to check out the linkage, if any, between the localized shear deformation and/or microcracking with the IPE events that occur in the present CNCs. In addition, a new concept of damage resistance is introduced for the first time in the present work to explain the presence of a strong indentation size effect (ISE) in the 40 ZTA CNCs. Finally, an attempt is also directed to understand how the indentation load (P) controls the relative size of interaction zones of dislocation loops as well as the damage resistance and thereby, engineer the acuteness of the ISE in ZTA CNCs. The implication of these findings in futuristic design of especially the ZTA CNCs for various applications is also discussed. 相似文献
22.
Size-dependent separation of graphene oxide by deformation of packed-gel in a chromatographic column
Yuji Takaoka Shohei Esaki Koichi Sakaguchi Tomotsumi Fujisawa Masashi Unno Shintaro Morisada 《分离科学与技术》2020,55(7):1356-1363
ABSTRACTA deformable gel-packed chromatographic column was used to separate as-synthesized graphite oxide with different sizes. The synthesized gel (56 µm) was deformed by pressure of the fluid flow and the gaps in the gels showed a range of sizes. A suspension of graphene oxide (0.1 g/L, 10 mL) was injected, and graphene oxide in the elution had a size at 0.56 μm and 0.14 μm, whereas in half upper and bottom domain of the gel layer graphene oxide had a size at 33 µm and 2.9 µm, respectively, demonstrating that graphene oxide suspension was separated by size through gel layer. 相似文献
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Bharti M. Shinde 《热应力杂志》2020,43(10):1234-1257
Abstract In the present study, thermoelastic analysis of laminated composite and sandwich shells (cylindrical/spherical) is presented using fifth-order shear and normal deformation theory. The significant characteristic of the present theory is that it includes the effects of both transverse shear and normal deformations. The mathematical formulation uses the principle of virtual work to derive the variationally consistent governing equations and traction free boundary conditions. To obtain the static solution, these governing equations are solved by employing Navier’s solution technique. The shell is subjected to a mechanical/thermal load sinusoidally distributed over the top surface of the shell. The thermal load linearly varies across the thickness of the shell. The present results are compared with other higher-order models and 3D elasticity solution wherever possible. Thermal stresses presented in this study will act as a benchmark for the future work. 相似文献
25.
153301工作面受上部3煤和9煤采空区及煤柱影响,巷道围岩变形量大。采用FLAC3D软件分别模拟不同锚杆间距和数量下的巷道围岩变形量,得到锚杆最优支护参数。针对153301工作面巷道采用锚网索和二次注浆加固支护技术,分别设计了不同的支护参数,并对支护后围岩变形量进行监测,监测结果表明围岩变形量和变形速率都有了明显的减小,支护取得了良好的效果。 相似文献
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通过Gleeble3500热模拟试验机进行热压缩试验并结合微观组织观察和统计分析,研究了热变形对GH4169合金中NbC颗粒尺寸形貌、分布特征的影响规律。研究表明压缩过程中的绝热效应会导致试样心部温度的进一步升高,从而为变形过程中的NbC回溶提供条件。NbC颗粒与基体在变形过程中形成的高位错密度区促进了元素的扩散,并加速了小曲率半径的尖角区域回溶和钝化。随变形量的增加NbC回溶趋势增加,其平均尺寸与体积分数均呈降低趋势。变形过程金属流动会促进NbC颗粒的位移,在70%的变形量下,NbC颗粒平均间距增加趋势显著高于30%和50%变形量试样。因此随变形量的增加,NbC颗粒有从链状→链条弯曲→链条方向改变→弥散分布的分布特征,促进基体中原链状NbC呈细小、弥散分布。研究结果为GH4169闪光焊接性能的提高提供了直接的参考。 相似文献
29.
《中国有色金属学会会刊》2020,30(3):710-726
Cylindrical samples of Ni-based GH4037 alloy were compressed at solid temperatures (1200, 1250 and 1300 °C) and semi-solid temperatures (1340, 1350, 1360, 1370 and 1380 °C) with different strain rates of 0.01, 0.1 and 1 s−1. High temperature deformation behavior and microstructure evolution of GH4037 alloy were investigated. The results indicated that flow stress decreased rapidly at semi-solid temperatures compared to that at solid temperatures. Besides, the flow stress continued to increase after reaching the initial peak stress at semi-solid temperatures when the strain rate was 1 s−1. With increasing the deformation temperature, the size of initial solid grains and recrystallized grains increased. At semi-solid temperatures, the grains were equiaxed, and liquid phase existed at the grain boundaries and inside the grains. Discontinuous dynamic recrystallization (DDRX) characterized by grain boundary bulging was the main nucleation mechanism for GH4037 alloy. 相似文献
30.
《中国有色金属学会会刊》2020,30(9):2394-2412
TiC nanoparticle-reinforced Mg−4Zn−0.5Ca matrix nanocomposites were processed by combining multidirectional forging (MDF) and extrusion (EX). The grain size of the nanocomposite after MDF+EX multi-step deformation was significantly decreased compared with that processed only by MDF. The average size of the recrystallized grains gradually increased after EX with increasing the number of MDF passes at 270 °C. However, the grain size significantly decreased by MDF processing at 310 °C. Both fine and coarse MgZn2 phases appeared in the (MDF+EX)-processed nanocomposites, and their volume fractions gradually increased with increasing the number of MDF passes before EX. Ultrahigh tensile properties (yield strength of ~404 MPa, ultimate tensile strength of ~450.3 MPa and elongation of ~5.2 %) were obtained in the nanocomposite after three MDF passes at 310 °C followed by EX. This was attributed to the refinement of the recrystallized grains, together with the improved Orowan strengthening provided by the precipitated MgZn2 particles that were generated by MDF+EX multi-step deformation. 相似文献